5,5-二甲基-2-苯基-1,3-二恶烷合成路线 （共 25 条）
反应条件
1: 87 percent / water; acetone / mesoporous aluminosilicate / 0.5 h / 55 °C
2: 80 percent / mesoporous aluminosilicate / CH2Cl2 / 6 h / 45 °C
View Scheme
参考文献
Robinson, Mathew W.C.; Graham, Andrew E.
Tetrahedron Letters, 2007 , vol. 48, # 27 p. 4727 - 4731
反应条件
polystyrene divinyl benzene sulfonic acid in dichloromethane
T=20 - 50°C; chemoselective reaction;
参考文献
Verma, Sanjeev K.; Sathe, Manisha; Kaushik
Synthetic Communications, 2010 , vol. 40, # 11 p. 1701 - 1707
反应条件
in diethyl ether
8 h; Heating;
参考文献
Walther, H.; Haase, L.; Gross, H.; Costisella, B.; Keitel, I.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 6 p. 902 - 908
反应条件
1: indium trifluoromethanesulfonate / dichloromethane / 0.08 h / 20 °C
2: indium trifluoromethanesulfonate / 0.5 h / 20 °C / Neat (no solvent)
View Scheme
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
反应条件
1: diethyl ether / 6 h / Ambient temperature
2: 58 percent / diethyl ether / 8 h / Heating
View Scheme
参考文献
Walther, H.; Haase, L.; Gross, H.; Costisella, B.; Keitel, I.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 6 p. 902 - 908
反应条件
oxygen in benzene
T=290°C; Catalytic oxidation; isomerization; 6 h; Product distribution; Further Variations:CatalystsTemperatures;
参考文献
Fischer, Jutta; Hoelderich, Wolfgang F.
Journal of Catalysis, 2000 , vol. 194, # 2 p. 294 - 300
反应条件
in dichloromethane
T=20°C; 3 h;
参考文献
Chalova, O. B.; Kurmaeva, E. S.; Kantor, E. A.; Kiladze, T. K.; Rakhmankulov, D. L.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1434 - 1437
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1640 - 1644
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether; dichloromethane
Heating;
参考文献
Mukaiyama, Teruaki; Shiina, Isamu; Sakata, Kaku; Emura, Takayuki; Seto, Keitarou; Saitoh, Masahiro
Chemistry Letters, 1995 , # 3 p. 179 - 180
反应条件
3,3-dimethyldioxirane
参考文献
Akbalina; Zlotskii; Kabal'nova; Grigor'ev; Kotlyar; Shereshovets
Russian Journal of Applied Chemistry, 2002 , vol. 75, # 7 p. 1120 - 1122
反应条件
1-oxyl-2,2,5,5-tetramethyl-4-phenyl-Δ3-imidazoline 3-oxide; chlorine dioxide; potassium bromide in acetonitrile
T=35°C; 4 h; KineticsProduct distribution; Further Variations:TemperaturesReagents;
参考文献
Abdrakhmanova; Kabal'nova; Rol'nik; Yagafarova; Shereshovets
Russian Chemical Bulletin, 2004 , vol. 53, # 8 p. 1755 - 1760
