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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
77638-62-1
合成路线
（共 10 条）
77638-57-4
→
反应条件
77638-62-1
反应条件
trichlorophosphate in toluene Heating;
参考文献
Oikawa, Yuji; Tanaka, Masahide; Hirasawa, Hitoshi; Yonemitsu, Osamu
Heterocycles, 1981 , vol. 15, # 1 p. 207 - 212
65837-19-6
→
反应条件
77638-62-1
反应条件
1: 97 percent 2: 82 percent / AcOH / xylene / Heating 3: 98 percent / TsOH 4: 97 percent / NaOMe, ammonia / methanol 5: 94 percent / TsCl 6: LiAlH4 7: Heating 8: 92 percent / POCl3 / toluene / Heating View Scheme
参考文献
Oikawa, Yuji; Tanaka, Masahide; Hirasawa, Hitoshi; Yonemitsu, Osamu
Heterocycles, 1981 , vol. 15, # 1 p. 207 - 212
65837-15-2
→
反应条件
77638-62-1
反应条件
1: 81 percent / TsOH / tetrahydrofuran; benzene / 60 °C 2: 97 percent 3: 82 percent / AcOH / xylene / Heating 4: 98 percent / TsOH 5: 97 percent / NaOMe, ammonia / methanol 6: 94 percent / TsCl 7: LiAlH4 8: Heating 9: 92 percent / POCl3 / toluene / Heating View Scheme
参考文献
Oikawa, Yuji; Tanaka, Masahide; Hirasawa, Hitoshi; Yonemitsu, Osamu
Heterocycles, 1981 , vol. 15, # 1 p. 207 - 212
65837-23-2
→
反应条件
77638-62-1
反应条件
1: 82 percent / AcOH / xylene / Heating 2: 98 percent / TsOH 3: 97 percent / NaOMe, ammonia / methanol 4: 94 percent / TsCl 5: LiAlH4 6: Heating 7: 92 percent / POCl3 / toluene / Heating View Scheme
参考文献
Oikawa, Yuji; Tanaka, Masahide; Hirasawa, Hitoshi; Yonemitsu, Osamu
Heterocycles, 1981 , vol. 15, # 1 p. 207 - 212
67996-15-0
→
反应条件
77638-62-1
反应条件
1: 88 percent / NaH 2: 81 percent / TsOH / tetrahydrofuran; benzene / 60 °C 3: 97 percent 4: 82 percent / AcOH / xylene / Heating 5: 98 percent / TsOH 6: 97 percent / NaOMe, ammonia / methanol 7: 94 percent / TsCl 8: LiAlH4 9: Heating 10: 92 percent / POCl3 / toluene / Heating View Scheme
参考文献
Oikawa, Yuji; Tanaka, Masahide; Hirasawa, Hitoshi; Yonemitsu, Osamu
Heterocycles, 1981 , vol. 15, # 1 p. 207 - 212
77638-54-1
→
反应条件
77638-62-1
反应条件
1: 97 percent / NaOMe, ammonia / methanol 2: 94 percent / TsCl 3: LiAlH4 4: Heating 5: 92 percent / POCl3 / toluene / Heating View Scheme
参考文献
Oikawa, Yuji; Tanaka, Masahide; Hirasawa, Hitoshi; Yonemitsu, Osamu
Heterocycles, 1981 , vol. 15, # 1 p. 207 - 212
77638-53-0
→
反应条件
77638-62-1
反应条件
1: 98 percent / TsOH 2: 97 percent / NaOMe, ammonia / methanol 3: 94 percent / TsCl 4: LiAlH4 5: Heating 6: 92 percent / POCl3 / toluene / Heating View Scheme
参考文献
Oikawa, Yuji; Tanaka, Masahide; Hirasawa, Hitoshi; Yonemitsu, Osamu
Heterocycles, 1981 , vol. 15, # 1 p. 207 - 212
77638-56-3
→
反应条件
77638-62-1
反应条件
1: LiAlH4 2: Heating 3: 92 percent / POCl3 / toluene / Heating View Scheme
参考文献
Oikawa, Yuji; Tanaka, Masahide; Hirasawa, Hitoshi; Yonemitsu, Osamu
Heterocycles, 1981 , vol. 15, # 1 p. 207 - 212
77638-55-2
→
反应条件
77638-62-1
反应条件
1: 94 percent / TsCl 2: LiAlH4 3: Heating 4: 92 percent / POCl3 / toluene / Heating View Scheme
参考文献
Oikawa, Yuji; Tanaka, Masahide; Hirasawa, Hitoshi; Yonemitsu, Osamu
Heterocycles, 1981 , vol. 15, # 1 p. 207 - 212
77638-62-1
→
反应条件
77638-64-3
反应条件
palladium on activated charcoal in decalin 4 h; Heating;
参考文献
Oikawa; Tanaka; Hirasawa; Yonemitsu
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 6 p. 1606 - 1614
