1-(2,2-二甲基四氢-2H-吡喃-4-基)-1-丙酮合成路线 (共 3 条)
反应条件
potassium dichromate; sulfuric acid
T=50°C; 4 h;
参考文献
Kuroyan, R. A.; Markosyan, A. I.; Engoyan, A. P.; Vartanyan, S. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 12 p. 2219 - 2221
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 12 p. 2591 - 2594
反应条件
1: 1) Magnesium, 3) 18percent hydrochloric acid / 2) Ether, 5 deg C, 4 h, 3) 0 deg C.
2: 79 percent / Potassium bichromate, 14percent sulfuric acid / 4 h / 50 °C
View Scheme
参考文献
Kuroyan, R. A.; Markosyan, A. I.; Engoyan, A. P.; Vartanyan, S. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 12 p. 2219 - 2221
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 12 p. 2591 - 2594
反应条件
1: 25percent Aq. sodium hydroxide / 1 h / 50 °C
2: Aq. hydrochloric acid / Heating
View Scheme
参考文献
Kuroyan, R. A.; Markosyan, A. I.; Engoyan, A. P.; Vartanyan, S. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 12 p. 2219 - 2221
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 12 p. 2591 - 2594