3-(2-羟基-2-丙基)苯酚合成路线 （共 16 条）
反应条件
1: 2M NaOH / tetrahydrofuran; H2O / 1.5 h / 0 °C 2: Na2S2O4 / ethyl acetate; H2O 3: 2M HCl / methanol / 1.25 h / 100 °C 4: 82 percent / NaIO3 / H2O; ethyl acetate / 0.25 h 5: 1M NaOH, H2 / Raney nickel / ethyl acetate / 5 h / 70 °C / 2067.2 Torr 6: NaIO4 / ethyl acetate; H2O / 0.17 h / Ambient temperature View Scheme
参考文献
Corey, Paul F.; Trimmer, Robert W.; Biddlecom, William G.
Angewandte Chemie, 1991 , vol. 103, # 12 p. 1694 - 1696
反应条件
boron trifluoride in dichloromethane
T=0 - 5°C;
参考文献
Cella, J. A.
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 2125 - 2130
反应条件
hydrogenchloride in toluene; phenol
参考文献
General Electric Company
Patent: US4460798 A1, 1984 ;
参考文献
Attia,S.Y. et al.
Journal of the American Chemical Society, 1977 , vol. 99, p. 3401 - 3408
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v. Auwers
Justus Liebigs Annalen der Chemie, 1917 , vol. 413, p. 304
反应条件
2: durch Verseifen mit alkoh. Lauge
View Scheme
参考文献
v. Auwers
Justus Liebigs Annalen der Chemie, 1917 , vol. 413, p. 304
参考文献
Attia,S.Y. et al.
Journal of the American Chemical Society, 1977 , vol. 99, p. 3401 - 3408
