5-(4-甲基苯基)缬草酸合成路线 （共 12 条）
反应条件
50 Pd/C; hydrogen in ethanol
T=50°C; 6 h;
参考文献
Asano, Masayoshi; Nakamura, Tsuyoshi; Sekiguchi, Yukiko; Mizuno, Yumiko; Yamaguchi, Takahiro; Kuroda, Takeshi; Tamaki, Kazuhiko; Nishi, Takahide
Tetrahedron Asymmetry, 2013 , vol. 24, # 8 p. 449 - 456
反应条件
Multistep reaction.;
参考文献
Jackson, Richard F. W.; Oates, Leslie J.; Block, Michael H.
Chemical Communications, 2000 , # 15 p. 1401 - 1402
反应条件
1: potassium tert-butylate / tetrahydrofuran; dichloromethane / 20 h / 0 - 20 °C
2: hydrogen; 50 Pd/C / ethanol / 6 h / 50 °C
View Scheme
参考文献
Asano, Masayoshi; Nakamura, Tsuyoshi; Sekiguchi, Yukiko; Mizuno, Yumiko; Yamaguchi, Takahiro; Kuroda, Takeshi; Tamaki, Kazuhiko; Nishi, Takahide
Tetrahedron Asymmetry, 2013 , vol. 24, # 8 p. 449 - 456
反应条件
potassium cyanide; ethanol
Erwaermen des Reaktionsprodukts mit wss. H2SO4;
参考文献
Huisgen; Vossius
Monatshefte fuer Chemie, 1957 , vol. 88, p. 517,527
反应条件
1: LiAlH4; diethyl ether
2: red phosphorus; concentrated sulfuric acid; aqueous hydrobromic acid
3: KCN; aqueous ethanol / Erwaermen des Reaktionsprodukts mit wss. H2SO4
View Scheme
参考文献
Huisgen; Vossius
Monatshefte fuer Chemie, 1957 , vol. 88, p. 517,527
反应条件
1: red phosphorus; concentrated sulfuric acid; aqueous hydrobromic acid
2: KCN; aqueous ethanol / Erwaermen des Reaktionsprodukts mit wss. H2SO4
View Scheme
参考文献
Huisgen; Vossius
Monatshefte fuer Chemie, 1957 , vol. 88, p. 517,527
反应条件
hydrogenchloride; mercury; zinc
Heating;
参考文献
Sen Gupta,S.C.; Sen,P.K.
Journal of the Indian Chemical Society, 1962 , vol. 39, # 10 p. 653 - 659
反应条件
1: AlCl3
2: Zn-Hg, aq. HCl / Heating
View Scheme
参考文献
Sen Gupta,S.C.; Sen,P.K.
Journal of the Indian Chemical Society, 1962 , vol. 39, # 10 p. 653 - 659
反应条件
1: AlCl3
2: Zn-Hg, aq. HCl / Heating
View Scheme
参考文献
Sen Gupta,S.C.; Sen,P.K.
Journal of the Indian Chemical Society, 1962 , vol. 39, # 10 p. 653 - 659
反应条件
aluminium trichloride
参考文献
Beyer
Chemische Berichte, 1937 , vol. 70, p. 1482,1489
