1,3-豆蔻酸二甘油酯(C14:0)合成路线 (共 16 条)
反应条件
trifluoroacetic acid in benzene 6 h; Heating; Equilibrium constant;
参考文献
Isai; Usol'tsev; Stiba
Chemistry of Natural Compounds, 2003 , vol. 39, # 4 p. 325 - 329
反应条件
Mucor javanicus lipase immobilised on nano-sized magnetite
T=60°C; P=760.051 Torr; 9 h; Molecular sieveEnzymatic reaction; regioselective reaction;
参考文献
Meng, Xiao; Xu, Gang; Zhou, Qin-Li; Wu, Jian-Ping; Yang, Li-Rong
Food Chemistry, 2014 , vol. 143, p. 319 - 324
反应条件
immobilized Candida antarctica lipase in dichloromethane
T=0 - 4°C; 5 h;
参考文献
Halldorsson, Arnar; Magnusson, Carlos D.; Haraldsson, Gudmundur G.
Tetrahedron, 2003 , vol. 59, # 46 p. 9101 - 9109
反应条件
glycerol
T=150 - 200°C;
参考文献
Hunter; Roberts; Kester
Journal of the American Chemical Society, 1948 , vol. 70, p. 3245,3246
反应条件
in dichloromethane
T=20°C;
参考文献
SEPS Pharma N.V.; GONNISSEN, Yves, Rene, Johanna, Paul
Patent: WO2010/115869 A1, 2010 ;
Location in patent: Page/Page column 25 ;
反应条件
sodium tetrahydroborate in tetrahydrofuran; water
T=0°C; 0.25 h; Title compound not separated from byproducts;
参考文献
Cockman, Samantha J.; Joll, Cynthia A.; Mortimer, Bok-Cheng; Redgrave, Trevor G.; Stick, Robert V.
Australian Journal of Chemistry, 1990 , vol. 43, # 12 p. 2093 - 2097
反应条件
sodium cyanoborohydride; acetic acid in tetrahydrofuran
0.5 h;
参考文献
Cockman, Samantha J.; Joll, Cynthia A.; Mortimer, Bok-Cheng; Redgrave, Trevor G.; Stick, Robert V.
Australian Journal of Chemistry, 1990 , vol. 43, # 12 p. 2093 - 2097
反应条件
quinoline; chloroform
unter Kuehlung und Kochen des Reaktionsgemisches mit Silbernitrit in verd.Alkohol;
参考文献
Averill; Roche; King
Journal of the American Chemical Society, 1929 , vol. 51, p. 869
反应条件
sodium methylate; xylene
und anschliessend mit Glycerin, jeweils bei 60grad;
参考文献
Baur; Lange
Journal of the American Chemical Society, 1951 , vol. 73, p. 3926
反应条件
HMS-TBD in dimethyl sulfoxide
T=110°C; 3 h;
参考文献
Kharchafi, Ghizlane; Jerome, Francois; Adam, Isabelle; Pouilloux, Yannick; Barrault, Joel
New Journal of Chemistry, 2005 , vol. 29, # 7 p. 928 - 934