4-(乙酰基氧基)-5,7-二甲氧基-2-萘羧酸甲酯合成路线 （共 12 条）
反应条件
1: 93 percent / potassium carbonate; methanol / acetone / 3 h / 35 °C 2: potassium carbonate / acetone / 16 h / Heating 3: LiAlH4 / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Piettre, Arnaud; Chevenier, Emmanuel; Massardier, Christine; Gimbert, Yves; Greene, Andrew E.
Organic Letters, 2002 , vol. 4, # 18 p. 3139 - 3142
反应条件
1: 82 percent / benzene / 288 h / 20 °C
2: 63 percent / potassium acetate / 0.25 h / Heating
View Scheme
参考文献
Piettre, Arnaud; Chevenier, Emmanuel; Massardier, Christine; Gimbert, Yves; Greene, Andrew E.
Organic Letters, 2002 , vol. 4, # 18 p. 3139 - 3142
反应条件
potassium acetate
0.166667 h; Heating;
参考文献
Rizzacasa, Mark A.; Sargent, Melvyn V.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1737 - 1743
反应条件
boron trichloride in dichloromethane
T=0°C; 7.25 h; Title compound not separated from byproducts;
参考文献
Carvalho, Christopher F.; Russo, Albert V.; Sargent, Melvyn V.
Australian Journal of Chemistry, 1985 , vol. 38, # 5 p. 777 - 792
反应条件
sodium acetate
6 h; Heating;
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.
Australian Journal of Chemistry, 1980 , vol. 33, # 11 p. 2531 - 2541
反应条件
1: 100 percent / 90percent trifluoroacetic acid / 0.17 h / Ambient temperature
2: 96 percent / potassium acetate / 0.17 h / Heating
View Scheme
参考文献
Rizzacasa, Mark A.; Sargent, Melvyn V.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1737 - 1743
反应条件
pyridine; boron trichloride
1.) dichloromethane, 0 deg, 7,25 h, 2.) RT, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carvalho, Christopher F.; Russo, Albert V.; Sargent, Melvyn V.
Australian Journal of Chemistry, 1985 , vol. 38, # 5 p. 777 - 792
反应条件
1: 93 percent / potassium carbonate; methanol / acetone / 3 h / 35 °C
2: potassium carbonate / acetone / 16 h / Heating
View Scheme
参考文献
Piettre, Arnaud; Chevenier, Emmanuel; Massardier, Christine; Gimbert, Yves; Greene, Andrew E.
Organic Letters, 2002 , vol. 4, # 18 p. 3139 - 3142
反应条件
sodium hydroxide
1 h; Heating;
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.
Australian Journal of Chemistry, 1980 , vol. 33, # 11 p. 2531 - 2541
反应条件
mercury(II) diacetate; iodine in acetic acid
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; Pannan, Linda J. H.; Raston, Colin L.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 610 - 627
