4,4-二丁基-γ-丁内酮合成路线 (共 4 条)
反应条件
[Ti(tert-butoxide)4] in dichloromethane
T=20°C; 18 h;
参考文献
Nakamura,E.; Oshino,H.; Kuwajima,I.
Journal of the American Chemical Society, 1986 , vol. 108, p. 3745
反应条件
potassium permanganate; (benzyl)-tri-(butyl)-ammonium chloride in water; benzene
48 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Lehmann, Jochen; Marquardt, Norbert
Synthesis, 1987 , # 12 p. 1064 - 1067
反应条件
in ethanol; sulfuric acid
T=30°C; electrochemical reaction: mercury pool cathode, platinum anode;
参考文献
Prasad; Misra
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 4 p. 392 - 393
反应条件
sulfuric acid
1.) electrochemical reaction: mercury pool cathode, platinum anode, H2SO4, ethanol, H2O, 30 deg C, 2.) reflux, 5-6 h; Yield given. Multistep reaction;
参考文献
Prasad; Misra
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 4 p. 392 - 393