苄基2,2,2-三氟乙基硫醚合成路线 (共 10 条)
反应条件
sodium hydroxide in water; N,N-dimethyl-formamide
参考文献
Bunyagidj, Chaiyun; Piotrowska, Hanna; Aldridge, Mary H.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3335 - 3336
反应条件
in N-methyl-acetamide; water
反应条件
sodium isopropanolate in isopropyl alcohol 48 h; HeatingNaOMe in MeOH, 20 h , reflux;
参考文献
Langler, Richard Francis; Morrison, Nancy Ann
Canadian Journal of Chemistry, 1987 , vol. 65, p. 2385 - 2389
反应条件
sodium methylate in methanol 20 h; Heating; Yield given. Yields of byproduct given;
参考文献
Canadian Journal of Chemistry, , vol. 65, p. 2385 - 2389
反应条件
1: 67 percent / 30percent H2O2 / acetic acid / 67 h 2: 93 percent / 1 M NaOH / dioxane / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 61, # 21 p. 7250 - 7255
反应条件
chlorine in water T=-5 - 0°C; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 46, # 16 p. 3335 - 3336
反应条件
phosphorus pentoxide T=150 - 180°C;
参考文献
Russian Chemical Bulletin, , vol. 55, # 7 p. 1200 - 1208
反应条件
chlorine in hydrogenchloride T=-30 - -25°C; 0.5 h;
参考文献
Chemische Berichte, , vol. 121, p. 1435 - 1440
反应条件
chlorine in water T=-5 - 0°C; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 46, # 16 p. 3335 - 3336
反应条件
chlorine in various solvent(s)
T=5°C; 0.5 h;
参考文献
Fritz, Helmut; Sundermeyer, Wolfgang
Chemische Berichte, 1989 , vol. 122, p. 1757 - 1764