[(1R,4S)-4-(羟基甲基)-1-环戊-2-烯基]氯化铵合成路线 （共 5 条）
反应条件
lithium triethylborohydride in tetrahydrofuran
T=0°C; 0.5 h;
参考文献
Kam, Bernard L.; Oppenheimer, Norman J.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3268 - 3272
反应条件
1: 98 percent / HCl / methanol / 1 h / Heating
2: 95 percent / Lithium triethylborohydride / tetrahydrofuran / 0.5 h / 0 °C
View Scheme
参考文献
Kam, Bernard L.; Oppenheimer, Norman J.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3268 - 3272
反应条件
1: 90 percent / 1N HCl / H2O / 1 h / Heating
2: 98 percent / HCl / methanol / 1 h / Heating
3: 95 percent / Lithium triethylborohydride / tetrahydrofuran / 0.5 h / 0 °C
View Scheme
参考文献
Kam, Bernard L.; Oppenheimer, Norman J.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3268 - 3272
反应条件
1: 95 percent / pyridine / 24 h / 0 °C
2: DBU / CHCl3 / 1 h / 0 °C
3: 0.163 g / K2CO3 / p-xylene / 14 h / Heating
4: 89 percent / HCl / methanol / 24 h / Heating
View Scheme
参考文献
An, Gwang-Il; Rhee, Hakjune
Nucleosides, Nucleotides and Nucleic Acids, 2002 , vol. 21, # 1 p. 65 - 72
反应条件
in pyridine
Yield given;
参考文献
Kam, Bernard L.; Oppenheimer, Norman J.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3268 - 3272
