5-硝基-1H-异色烯-1-酮合成路线 （共 16 条）
反应条件
1: dimethylformamide / 16 h / 150 °C
2: SiO2 / ethyl acetate
View Scheme
参考文献
Wong, See-Mun; Shah, Bhavini; Shah, Priyal; Butt, Ian C.; Woon, Esther C.Y.; Wright, James A.; Thompson, Andrew S.; Upton, Christopher; Threadgill, Michael D.
Tetrahedron Letters, 2002 , vol. 43, # 12 p. 2299 - 2302
反应条件
in N,N-dimethyl-formamide
12 h; Heating;
参考文献
Somei; Karasawa; Shoda; Kaneko
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 1 p. 249 - 253
反应条件
1.) DMF, reflux, 10 h; 2.) water; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Somei; Karasawa; Shoda; Kaneko
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 1 p. 249 - 253
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in tetrahydrofuran
6 h;
参考文献
Parveen, Ifat; Naughton, Declan P.; Whish, William J. D.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 14 p. 2031 - 2036
反应条件
in methanol
1 h; Heating;
参考文献
Somei; Karasawa; Shoda; Kaneko
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 1 p. 249 - 253
反应条件
1: 41.3 percent / concd. hydrochloric acid / 6.5 h / Heating
2: 86.3 percent / methanol / 1 h / Heating
View Scheme
参考文献
Somei; Karasawa; Shoda; Kaneko
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 1 p. 249 - 253
