戊-4-炔基对甲苯磺酸酯合成路线 (共 17 条)
参考文献
Atkinson, Robert S.; Grimshire, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1215 - 1224
反应条件
in methanol Heating;
参考文献
Luo, Fen-Tair; Wang, Ren-Tzong
Tetrahedron Letters, 1992 , vol. 33, # 45 p. 6835 - 6838
反应条件
acetone Ansaeuern der Reaktionsloesung;
参考文献
Eglinton; Whiting
Journal of the Chemical Society, 1953 , p. 3052,3055
反应条件
sodium iodide in acetone
T=70°C; 1 h;
参考文献
Tashima, Toshihiko; Toriumi, Yoshimi; Mochizuki, Yumi; Nonomura, Taro; Nagaoka, Satoru; Furukawa, Katsuo; Tsuru, Hiromichi; Adachi-Akahane, Satomi; Ohwada, Tomohiko
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 23 p. 8014 - 8031
反应条件
potassium carbonate in acetone
2 h; RefluxInert atmosphere;
参考文献
Lu, Biao; Li, Yuxue; Wang, Youliang; Aue, Donald H.; Luo, Yingdong; Zhang, Liming
Journal of the American Chemical Society, 2013 , vol. 135, # 23 p. 8512 - 8524
反应条件
1: ethyl acetoacetate With sodium hydride; potassium iodide in tetrahydrofuran; N,N-dimethyl-formamide
T=0 - 20°C;
2: 4-pentynyl tosylate in tetrahydrofuran; N,N-dimethyl-formamide
T=20 - 100°C;
参考文献
Deng, Chen-Liang; Song, Ren-Jie; Liu, Yi-Lin; Li, Jin-Heng
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 18 p. 3096 - 3100
反应条件
ethanol; sodium ethanolate
参考文献
Eglinton; Whiting
Journal of the Chemical Society, 1950 , p. 3650,3655