2,3-二氢-4(1H)-菲酮合成路线 （共 49 条）
参考文献
Journal of the American Chemical Society, , vol. 67, p. 1745,1752
反应条件
Erhitzen des Chlorids auf 130-140grad;
参考文献
Chemische Berichte, , vol. 62, p. 649
参考文献
Journal of the Chemical Society, , p. 1125,1131
参考文献
Chemische Berichte, , vol. 62, p. 649
反应条件
1: amalgamated zinc; aqueous HCl 2: AlCl3; dinitrobenzene / -10 °C 3: amalgamated zinc; concentrated aqueous HCl; acetic acid / weiteres Reagens: Toluol 4: palladium coal / 300 - 320 °C View Scheme
参考文献
Bachmann; Struve
Journal of Organic Chemistry, 1939 , vol. 4, p. 472,477
Journal of Organic Chemistry, 1940 , vol. 5, p. 416,420, 427
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran
参考文献
Feringa,B.; Wynberg,H.
Recueil des Travaux Chimiques des Pays-Bas, 1978 , vol. 97, p. 249 - 252
反应条件
1: N2H4*H2O, aq. HCl / ethanol / Heating 2: Pd-C View Scheme
参考文献
Dewar,M.J.S.; Poesche,W.H.
Journal of Organic Chemistry, 1964 , vol. 29, p. 1757 - 1762
反应条件
1.1: n-butyllithium; N-cyclohexyl-N-isopropylamine / tetrahydrofuran; hexane / -78 °C / Inert atmosphere 1.2: 1 h / -78 °C / Inert atmosphere 2.1: palladium 10 on activated carbon / triglyme (triethylene glycol dimethyl ether) / 4 h / 240 °C / Inert atmosphere 3.1: diisobutylaluminium hydride / hexane; toluene / 1 h / -78 °C / Inert atmosphere 3.2: Inert atmosphere 4.1: methanesulfonic acid / dichloromethane / 0.5 h / 20 °C / Cooling with ice View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
反应条件
1: NaBH4 / methanol 2: HCl-AcOH 3: 44 percent Spectr. / H2 / Pd/C / diethyl ether / 24 h / 25 °C View Scheme
参考文献
Ernst, Ludger; Stolle, Ralf
Magnetic Resonance in Chemistry, 1989 , vol. 27, # 8 p. 796 - 797
参考文献
Linstead; Michaelis
Journal of the Chemical Society, 1940 , p. 1134,1138
