1: With (-) planar-chiral PPY derivative Fe in toluene T=20°C; 1.5 h; 2: With lithium hydroxide; dihydrogen peroxide in tetrahydrofuran; water T=0°C; 1.5 h; 3: With sodium carbonate; sodium thiosulfate in tetrahydrofuran; water T=20°C; 0.25 h; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 124, # 34 p. 10006 - 10007
Nocardia diaphanozonaria cells; glycerol; peptone; beef extract; yeast extract in water T=30°C; pH=7.0; 48 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 68, # 19 p. 7234 - 7242
1: With (R)-BINOL-SnCl4 in dichloromethane; toluene T=-78°C; enantioselective protonation; 1 h; 2: With hydrogenchloride in dichloromethane; toluene Hydrolysis; Further stages. Title compound not separated from byproducts.;
参考文献
Journal of the American Chemical Society, , vol. 122, # 34 p. 8120 - 8130