1: With hydrogen; CN; palladium on activated charcoal in ethyl acetate 1 h; 2: With sodium hydroxide; bromine in 1,4-dioxane; water 3 h; 3: With sodium sulfite in 1,4-dioxane; water Title compound not separated from byproducts;
参考文献
European Journal of Organic Chemistry, , # 23 p. 3986 - 3994
Birman's catalyst; benzoic acid anhydride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 12 h; Resolution of racemate; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 35 p. 5887 - 5890
Birman's catalyst; benzoic acid anhydride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 11 h; Resolution of racemate; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 35 p. 5887 - 5890
water; Candida rugosa lipase in cyclohexane T=45°C; 5 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 66, # 1-2 p. 113 - 119
water; Candida rugosa lipase in cyclohexane T=45°C; 5 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 66, # 1-2 p. 113 - 119
