in neat (no solvent) 0.5 atm F2; slow reaction at room temp., instantaneous at 50-70°C;
参考文献
Butskii, V. D.; Pervov, V. S.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1977 , vol. 22, p. 6 - 8
Zhurnal Neorganicheskoi Khimii, 1977 , vol. 22, p. 14 - 17
in neat (no solvent) WTe2 placed in a tungsten saucer, addn. of a small amt. of sulfur as fuse, react. with fluorine in a prefluorinated perforated nickel crucible;
参考文献
O'Hare, P. A. G.; Hope, G. A.
Journal of Chemical Thermodynamics, 1992 , vol. 24, # 6 p. 639 - 647
in neat (no solvent) Ensemble of MoTe2 on W-saucer with small quantities of S, resting on a perfluorinated Ni-crucible, is combusted with F2 in a calorimeter bomb.; Gases are condensed into a trap (liq. N2).;
参考文献
O'Hare, P. A. G.; Hope, G. A.
Journal of Chemical Thermodynamics, 1989 , vol. 21, # 7 p. 701 - 708
