in neat (no solvent) heating in cooled copper tube (water) to 650°C; description of apparatus given;; condensed (liquid O2); passed through flasks containing H2O and hot aq. KOH; dried over P2O5;;
参考文献
S: MVol.B3, 83, page 1712 - 1714
Brauer, G., Handbuch der praeparativen anorganischen Chemie, 2. Aufl., Bd. 1, Stuttgart 1960, S. 166
Brauer, G., Handbuch der praeparativen anorganischen Chemie, Stuttgart 1954, S. 140
in neat (no solvent) dry apparatus, free of air (SO2 atm.); glowing platinum wire;; storage (several hours/over H2O); washing with H2O (removal of SOF2/SO2); dried (molten KF); cooled (-80°C); removal of O2 (pump);;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 132, p. 374 - 381
