in neat (no solvent) N3F and an excess of F2 at 80°C;;
参考文献
Gmelin Handbook: F: SVol.1, 72, page 247 - 248
Full Text Show Details
Haller, J. F.
Diss. Cornell Univ. 1942
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反应条件
in neat (no solvent) a mixt. of a small excess of F2 and HN3 dild. with N2 is passed through a spiral tube of copper into two cold traps (the first cooled with aceton/CO2, the second with liq. air);; ppt. in the second cold trap; fractional distn. (explosion possible);;
参考文献
Gmelin Handbook: F: SVol.1, 72, page 247 - 248
Full Text Show Details
Haller, J. F.
Diss. Cornell Univ. 1942
Ruff, O.; Fischer, J.; Luft, F.
Z. Anorg. Chem., 1928 , vol. 172, p. 417 - 428
Full Text Show Details
Gmelin Handbook: N: MVol.1, 1.4.2.41, page 250 - 250
