in neat (no solvent)
byproducts: O2; transport reaction: passing F2-N2 mixture over KClO3 at 25 - 60°C;; washing with NaOH; passing ClO3F through Na2S2O3 soln.; drying over NaOH and P2O5;;
参考文献
Engelbrecht, A.; Atzwanger, H.
Journal of Inorganic and Nuclear Chemistry, 1956 , vol. 2, p. 348 - 357
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Gmelin Handbook: Cl: SVol.B2, 125, page 579 - 581
in sodium hydroxide
byproducts: O2; aq. NaOH; F2 is passed through a Pt-tube in a 2percent aq. NaOH (1-2 l/h);; washing with H2O; condensation by liq. O2; fractional distn.; 98.5percent purity (one time distn.);;
参考文献
Brauer, G.
Handbuch der praeparativen anorganischen Chemie, Stuttgart 1954, S. 136/7
