in pyridine byproducts: TlBr; heated for 40 h in refluxing pyridine;
参考文献
Gun'kin, I. F.; Butin, K. P.; Beletskaya, I. P.; Reutov, O. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, p. 1781 - 1781
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , p. 2166 - 2166
in benzene-d6 vac. drybox or under N2 using Schlenk techniques; to soln. of (CyNC(Me)NCy)Ge(N(SiMe3)2)(SePh)2 in C6D6 selenium was added, heated at 60°C for 2 h;
参考文献
Foley, Stephen R.; Yap, Glenn P. A.; Richeson, Darrin S.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 10 p. 1663 - 1668
in neat (no solvent)
on heating in an autoclave to 265-290°C with an excess of Se;;
参考文献
Emeleus, H. J.
Fortschr. Chem. Forsch., 1951 , vol. 2, p. 609 - 618
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Emeleus, H. J.
Suomen Kemistilehti B, 1958 , vol. 31, p. 101 - 109
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Gmelin Handbook: C: MVol.D2, 4.2.4.4.5, page 319 - 320
Koshcheeva, L. S.; Lavrent'ev, A. N.; Sochilin, E. G
Zhurnal Obshchei Khimii, 1974 , vol. 44, p. 2069
Zhurnal Obshchei Khimii, 1974 , vol. 44, p. 2108
C.A., 1974 , vol. 81, p. 169046
in melt
sulphur and selenium were mixed together in molar ratio 70:30, 65:35, 60:40 heated in sealed ampules under reduced pressure (ca. 0.01 kPa) at 770 K for 4 h and quenched at liq. N2 temp.; further products; various product ratio for various conditions;; the resulting amorphous materials were extd. with CS2, after which the solvent was evapd.;;
参考文献
Chivers, Tristram; Laitinen, Risto S.; Schmidt, Kenneth J.
Canadian Journal of Chemistry, 1992 , vol. 70, # 3 p. 719 - 725
