硝酸铁(III) 九水合物合成路线 (共 31 条)
反应条件
in nitric acid Fe is dissolved in HNO3 (34percent, d =1.21), at the beginning Fe is dissolved quickly with evolution of gas, then slowly without evolution of gas and formation of Fe(NO3)3 and traces of NO2 and NH3;;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 112, p. 1451 - 1451
反应条件
in water addn. of 10 percent soln. of NH4OH to soln. of Fe-salt (pptn.), filtration, washing (hot water) to remove NH4(1+), and SO4(2-), redissolving of Fe(OH)3 in 0.5 M HNO3;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 42, # 10 p. 1552 - 1556
反应条件
potassium hydroxide; oxygen in water 3 ml of 11 M KOH soln. contg. Fe(NO3)3 and K3Fe(CN)6 were placed in bubbler and O2 was passed through, HCl was added;
参考文献
Shilov; Gogolev
Russian Journal of General Chemistry, 2009 , vol. 79, # 9 p. 1773 - 1777
反应条件
in neat (no solvent) byproducts: FeCl2; Fe(NO3)3 is heated for a longer time to 110 - 120°C in a HCl strea, formation of FeCl3, contaminated with some FeCl2;;
参考文献
Jannasch, P.; Schmidt, F.
Z. Anorg. Chem., 1895 , vol. 9, p. 278 - 278
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Jannasch, P.; Schmidt, F.
Z. Anorg. Chem., 1895 , vol. 9, p. 281 - 281
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Gmelin Handbook: Fe: MVol.B1, 98, page 221 - 223
反应条件
ammonium chloride; ammonia in water
参考文献
Imperial Chemical Industries Limited
Patent: US4048180 A1, 1977 ;
反应条件
ammonium chloride in ammonia
参考文献
Imperial Chemical Industries Limited
Patent: US4048180 A1, 1977 ;
反应条件
ammonium chloride; ammonia in diethyl ether
参考文献
Imperial Chemical Industries Limited
Patent: US4048180 A1, 1977 ;
反应条件
hydrogen in neat (no solvent) byproducts: NOx; sample inserted in U-shaped TPR cell and reduced in flow of 10 percent H2 in N2 by gradually raising system temp. to 1000 K at 5 K/min; T(r) is 465+/-20 K;
参考文献
Yuvaraj, Shanmugam; Lin, Fan-Yuan; Chang, Tsong-Huei; Yeh, Chuin-Tih
Journal of Physical Chemistry B, 2003 , vol. 107, # 4 p. 1044 - 1047
反应条件
ammonium chloride; ammonia; lithium in water
反应条件
ammonia; lithium in water
参考文献
Toray Industries
Patent: US4880939 A1, 1989 ;