N,N'-二-叔丁氧羰基-(L)-胱氨酸二甲酯合成路线 （共 19 条）
反应条件
tris-(dimethylamino)-phosphine in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Wang, Hua; Zhang, Jiming; Xian, Ming
Journal of the American Chemical Society, 2009 , vol. 131, # 37 p. 13238 - 13239
反应条件
sodium hydroxide in 1,4-dioxane; water
24 h; Ambient temperature;
参考文献
Ottenheijm, Harry C.J.; Liskamp, Rob M.J.; Nispen, Simon P.J.M. van; Boots, Hans A.; Tijhuis, Marian W.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3273 - 3283
反应条件
1: With tri-n-butyl-tin hydride; acetic acid; bis-triphenylphosphine-palladium(II) chloride in dichloromethane
T=20°C; deprotection; 0.5 h;
2: With iodine in tetrachloromethane
Oxidation;
参考文献
Kimbonguila, Andre Malanda; Merzouk, Ahmed; Guibe, Francois; Loffet, Albert
Tetrahedron, 1999 , vol. 55, # 22 p. 6931 - 6944
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; 30 h;
参考文献
Alfaro, Joshua F.; Zhang, Tiao; Wynn, DonRaphael P.; Karschner, Erin L.; Zhaohui, Sunny Zhou
Organic Letters, 2004 , vol. 6, # 18 p. 3043 - 3046
反应条件
oxygen; O-(2,4,6-trimethylbenzenesulfonyl)hydroxylamine; potassium carbonate in water; N,N-dimethyl-formamide
T=20°C; 0.0333333 h;
参考文献
Bernardes, Goncalo J. L.; Chalker, Justin M.; Errey, James C.; Davis, Benjamin G.
Journal of the American Chemical Society, 2008 , vol. 130, # 15 p. 5052 - 5053
反应条件
[BnEt3N]2MoS4 in acetonitrile
T=28°C;
参考文献
Bhat, Ramakrishna G.; Porhiel, Emmanuel; Saravanan, Vadivelu; Chandrasekaran, Srinivasan
Tetrahedron Letters, 2003 , vol. 44, # 28 p. 5251 - 5253
反应条件
triethylamine in dichloromethane
T=0 - 20°C; 3.25 h;
参考文献
Lin, Yuya A.; Chalker, Justin M.; Floyd, Nicola; Bernardes, Goncalo J. L.; Davis, Benjamin G.
Journal of the American Chemical Society, 2008 , vol. 130, # 30 p. 9642 - 9643
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Chalker, Justin M.; Wood, Charlotte S. C.; Davis, Benjamin G.
Journal of the American Chemical Society, 2009 , vol. 131, # 45 p. 16346 - 16347
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; triphenylphosphine in dichloromethane
T=4°C; 1 h;
参考文献
Tanaka, Ken; Ajiki, Kaori
Tetrahedron Letters, 2004 , vol. 45, # 1 p. 25 - 27
反应条件
dihydrogen peroxide; methyltrioxorhenium (VII) in acetic acid
T=20°C;
参考文献
Lazzaro, Francesco; Crucianelli, Marcello; De Angelis, Francesco; Neri, Veronica; Saladino, Raffaele
Tetrahedron Letters, 2004 , vol. 45, # 50 p. 9237 - 9240
反应条件
tris(4-bromophenyl)ammoniumyl stibanate; sodium hydrogencarbonate in acetonitrile
1 h;
参考文献
Platen, Martin; Steckhan, Eberhard
Liebigs Annalen der Chemie, 1984 , # 9 p. 1563 - 1576
