in neat (no solvent) condensing excess of H2S onto Ge-compd. at -196°C, warming to room temp., standing for 60 min; fractional low-temp. distn. (condensing at -196°C);
参考文献
Drake,J.E. et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 366 - 371
Hillel, R.; Bouix, J.; Forel, M.-T.
Bulletin de la Societe Chimique de France, 1974 , p. 83 - 88
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Gmelin Handbook: B: B Comp.SVol.1/3, 10.6.1.2, page 35 - 36
