反应条件
in hydrogen fluoride byproducts: H2, C5F12; Electrolysis; various electrodes; voltage: 5-6 V; current density: 0.02 A/cm*cm; amperage: <=2000 A; electrolysis of liq. HF at 0°C til formation of F2 then addn. of pyridine;; the formed gas is passed over NaF and then in a cold trap (acetone-CO2); dried; condensation in a cold trap (liq. air);;
参考文献
Journal of the Electrochemical Society, , vol. 95, p. 64 - 67
Journal of the Electrochemical Society, , vol. 95, p. 47 - 52
F: SVol.1, 67, page 238 - 240
US2490098 , ;
Diss. Muenchen 1955