trifluorophosphane合成路线 (共 187 条)
反应条件
in not given
react. with stoichiometric amounts of (CH3)3N;;
参考文献
Parry, R. W.; Bissot, T. C.
Journal of the American Chemical Society, 1956 , vol. 78, p. 1524 - 1527
反应条件
in acetonitrile
byproducts: KCl, HCl; PCl3 in MeCN was slowly added to a boiling suspn. of KHF2 in MeCN;; the gaseous prod. was condensed in trap cooled by liq. N2 and distd. at -100°C; elem. anal.; IR;
参考文献
Kalbandkeri, R. G.; Padma, D. K.; Vasudeva Murthy, A. R.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1984 , vol. 23, p. 990 - 991
反应条件
in acetonitrile
byproducts: KBr, HBr; PBr3 in MeCN was slowly added to a boiling suspn. of KHF2 in MeCN;; the gaseous prod. was condensed in trap cooled by liq. N2 and distd. at -100°C; elem. anal.; IR;
参考文献
Kalbandkeri, R. G.; Padma, D. K.; Vasudeva Murthy, A. R.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1984 , vol. 23, p. 990 - 991
反应条件
in gas
byproducts: NiC6H6(1+); The react. is performed on an ion cyclotron resonance (ICR) mass spectrometer. The nickel ion and the aromatic compd. are admitted to the ICR cell in approx. 1:1 ratio, to a total pressure of 6E-6 Torr.; MS;
参考文献
Stepnowski, Richard; Allison, John
Journal of the American Chemical Society, 1989 , vol. 111, # 2 p. 449 - 457
反应条件
in gas
byproducts: NiC6H5CH3(1+); The react. is performed on an ion cyclotron resonance (ICR) mass spectrometer. The nickel ion and the aromatic compd. are admitted to the ICR cell in approx. 1:1 ratio, to a total pressure of 6E-6 Torr.; MS;
参考文献
Stepnowski, Richard; Allison, John
Journal of the American Chemical Society, 1989 , vol. 111, # 2 p. 449 - 457
反应条件
in gas
byproducts: NiC6H5(CH2)3CH3(1+); The react. is performed on an ion cyclotron resonance (ICR) mass spectrometer. The nickel ion and the aromatic compd. are admitted to the ICR cell in approx. 1:1 ratio, to a total pressure of 6E-6 Torr.; MS;
参考文献
Stepnowski, Richard; Allison, John
Journal of the American Chemical Society, 1989 , vol. 111, # 2 p. 449 - 457
反应条件
in gas
byproducts: NiC6H5CN(1+); The react. is performed on an ion cyclotron resonance (ICR) mass spectrometer. The nickel ion and the aromatic compd. are admitted to the ICR cell in approx. 1:1 ratio, to a total pressure of 6E-6 Torr.; MS;
参考文献
Stepnowski, Richard; Allison, John
Journal of the American Chemical Society, 1989 , vol. 111, # 2 p. 449 - 457
反应条件
in gas
byproducts: NiC6H5CHO(1+); The react. is performed on an ion cyclotron resonance (ICR) mass spectrometer. The nickel ion and the aromatic compd. are admitted to the ICR cell in approx. 1:1 ratio, to a total pressure of 6E-6 Torr.; MS;
参考文献
Stepnowski, Richard; Allison, John
Journal of the American Chemical Society, 1989 , vol. 111, # 2 p. 449 - 457
反应条件
in gas
byproducts: NiC6H5Cl(1+); The react. is performed on an ion cyclotron resonance (ICR) mass spectrometer. The nickel ion and the aromatic compd. are admitted to the ICR cell in approx. 1:1 ratio, to a total pressure of 6E-6 Torr.; MS;
参考文献
Stepnowski, Richard; Allison, John
Journal of the American Chemical Society, 1989 , vol. 111, # 2 p. 449 - 457
反应条件
in gas
byproducts: NiC6H5Br(1+); The react. is performed on an ion cyclotron resonance (ICR) mass spectrometer. The nickel ion and the aromatic compd. are admitted to the ICR cell in approx. 1:1 ratio, to a total pressure of 6E-6 Torr.; MS;
参考文献
Stepnowski, Richard; Allison, John
Journal of the American Chemical Society, 1989 , vol. 111, # 2 p. 449 - 457