Schumb, W. C.; Anderson, H. H.
Journal of the American Chemical Society, 1937 , vol. 59, p. 651 - 653
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Gmelin Handbook: Si: MVol.B, 272, page 732 - 735
in neat (no solvent) addn. of SbF3 to a boiling soln. of Br2 free SiBr4 under stirring;; distillation;;
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Schumb, W. C.; Anderson, H. C.
Journal of the American Chemical Society, 1936 , vol. 58, p. 994 - 996
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Gmelin Handbook: Si: MVol.B, 271, page 730 - 732
antimony(V) pentachloride in neat (no solvent) byproducts: SiH4, HCl; at room temp. for 3 h; products distd. through two traps (-93°C, toluene slush, -130°C pentane slush), the second trap containing HSiF3 was isolated, evacuated for 30 min at -130°C (1.0 torr) to remove SiH4, HCl;
antimony pentachloride in neat (no solvent) byproducts: H2; conversion of 2.093g SiHCl3 with 0.5g SbF3 in presence of 0.2ml SbCl5 at 10-15 °C for a period of 3 hours;;
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Emeleus, H. J.; Maddock, A. G.
Journal of the Chemical Society, 1944 , p. 293 - 296
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Gmelin Handbook: Si: MVol.B, 233, page 635 - 638
in tetramethylene sulphone at 78-80°C; 48 h; condensation and fractionation; gas chromy.;
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Moule, D. C.; Subramaniam, C. R.
Canadian Journal of Chemistry, 1969 , vol. 47, p. 1011 - 1017
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Gmelin Handbook: F: PerFHalOrg.1, 1.1.1.2, page 8 - 9
