反应条件
in sulfur dioxide absence of moisture; mixing solns. of S4N4 and excess SbF5 (room temp.),standing for 48 h; filtration off of SbF3, crystn. (several months, room temp.), washing (liquid SO2), drying (reduced pressure);
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 971 - 974