Booth, H. S.; Carnell, P. H.
Journal of the American Chemical Society, 1946 , vol. 68, p. 2650 - 2652
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Gmelin Handbook: Si: MVol.C, 39, page 120 - 121
Emeleus; Heal
Journal of the Chemical Society, 1949 , p. 1697,1698
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Heal
Nature (London, United Kingdom), 1946 , vol. 158, p. 672
Chem.Abstr., 1947 , p. 947
Anderson
Journal of the American Chemical Society, 1947 , vol. 69, p. 2495
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Gmelin Handbook: P: MVol.C, 273, page 626 - 629
Na in ethanol; benzene
suspendion of SbF3 (20 mmol) in ethanol; addn. of a dithiolate soln. (formed on dissolving of 60 mmol Na in a mixture of 30 mmol ethanedithiole, ethanol and benzene) with stirring, refluxing and exclusion of moisture; heating for 1 h; hot filtration;; extraction of the residue with hot water; washing with ethanol; recrystallization from chloroform; elem. anal.;;
参考文献
Hoffmann, Harald M.; Draeger, Martin
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1986 , vol. 41, # 11 p. 1455 - 1460