Boc-1,5-二氨基戊烷盐酸盐合成路线 （共 6 条）
反应条件
chloroform; hydrogen; palladium on activated charcoal in methanol
P=1551.4 Torr; 1 h;
参考文献
Mattingly, Phillip G.
Synthesis, 1990 , p. 366 - 368
反应条件
triethylamine in tetrahydrofuran; methanol
1 h;
参考文献
Teshima, Tadashi; Matsumoto, Takahiro; Wakamiya, Tateaki; Shiba, Tetsuo; Aramaki, Yoshio; Nakajima, Terumi; Kawai, Nobufumi
Tetrahedron, 1991 , vol. 47, # 20-21 p. 3305 - 3312
反应条件
1: 100 percent / CH2Cl2 / 12 h
2: triethylamine / toluene / 0.08 h / 0 °C
3: NaN3 / tetrabutylammonium bromide / toluene; H2O / 3 h / 60 °C
4: 95 percent / H2, CHCl3 / Pd-C / methanol / 1 h / 1551.4 Torr
View Scheme
参考文献
Mattingly, Phillip G.
Synthesis, 1990 , p. 366 - 368
反应条件
1: 100 percent / CH2Cl2 / 12 h
2: triethylamine / toluene / 0.08 h / 0 °C
3: NaN3 / tetrabutylammonium bromide / toluene; H2O / 3 h / 60 °C
4: 95 percent / H2, CHCl3 / Pd-C / methanol / 1 h / 1551.4 Torr
View Scheme
参考文献
Mattingly, Phillip G.
Synthesis, 1990 , p. 366 - 368
反应条件
1: triethylamine / toluene / 0.08 h / 0 °C
2: NaN3 / tetrabutylammonium bromide / toluene; H2O / 3 h / 60 °C
3: 95 percent / H2, CHCl3 / Pd-C / methanol / 1 h / 1551.4 Torr
View Scheme
参考文献
Mattingly, Phillip G.
Synthesis, 1990 , p. 366 - 368
反应条件
1: NaN3 / tetrabutylammonium bromide / toluene; H2O / 3 h / 60 °C
2: 95 percent / H2, CHCl3 / Pd-C / methanol / 1 h / 1551.4 Torr
View Scheme
参考文献
Mattingly, Phillip G.
Synthesis, 1990 , p. 366 - 368
