in melt placing of mixt. of Al with SnF2 (molar ratio SnF2:Al=1.65) in Fluoroplast-4 ampule, closing by screwed stopper, exposition for 1.00 h at 250°C; various product ratio yields for various conditions; cooling, stirring up in water, collection, drying;
参考文献
Goryacheva; Rakov; Solov'ev
Russian Journal of Inorganic Chemistry, 2001 , vol. 46, # 7 p. 949 - 952
in neat (no solvent) byproducts: SOF2, HF; at 20°C; elem. anal., XRD;
参考文献
Shendrik, V. P.; Lyakh, O. D.; Yagupol'skii, L. M.
Sov. Prog. Chem. (Engl. Transl.), 1982 , vol. 48/10, p. 112 - 113
Ukrainskii Khimicheskii Zhurnal (Russian Edition), 1982 , vol. 48, p. 1108 - 1109
