in sulfur dioxide
condensing Cl2 onto Se, addn. of AsF5 and SO2 after 1 h, stirring (overnight); removal of volatiles; product mixture;
参考文献
Brownridge, Scott; Cameron, T. Stanley; Passmore, Jack; Schatte, Gabriele; Way, Todd C.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 12 p. 2553 - 2570
AsF5 condensed at -196°C onto a mixture of Br2 and AsBr3, warmed to -5°C, recooled to -196°C (repeated for more than 10 times); AsF3 removed at -5°C under dynamic vac.;
参考文献
Klapoetke, Thomas; Passmore, Jack; Awere, Edward G.
Journal of the Chemical Society, Chemical Communications, 1988 , # 21 p. 1426 - 1427
