反应条件
in tetrahydrofuran Irradiation (UV/VIS); (Ar) soln. Cr complex and diyne in THF was irradiated with Hg/Xe arc lamp (400-550 W) atb 210-600 nm for 6 h at room temp.; volatiles were removed in vacuo, residue was extd. with hexane, soln. was decanted and stored at -60°C overnight, soln. was filtered and evapd.; elem. anal.;
参考文献
Braunschweig, Holger; Herbst, Thomas; Rais, Daniela; Ghosh, Sundargopal; Kupfer, Thomas; Radacki, Krzysztof; Crawford, Andrew G.; Ward, Richard M.; Marder, Todd B.; Fernandez, Israel; Frenking, Gernot
Journal of the American Chemical Society, 2009 , vol. 131, # 25 p. 8989 - 8999