in gas heating SiHCl3 and H2 at 500°C in a reactor, passing over a Mg2Si charge which was heated upto 220°C, react. time: 4 h, condensing exit gases in liq. N2 traps; detn. by gas chromy., cooling the Mg2Si charge to room temp. under H2, deposition of Si on the reactor walls;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, , vol. 27, # 9 p. 756 - 758
