in tetrahydrofuran (under inert atm., Schlenk); C6H4CH3Sn(CH3)3 added to slurry of BiCl3 inTHF, refluxed for 2 h; solvent removed in vacuo, CH2Cl2 added, filtered; monitored by NMR;
参考文献
Mehring, Michael; Nolde, Christof; Schuermann, Markus
Inorganica Chimica Acta, 2009 , vol. 362, # 3 p. 745 - 752
Manulkin, Z. M.
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 2004 - 2008
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.4.7, page 73 - 76
in hydrogenchloride precipitation from an aq. hydrochloric solution of BiCl3 with concentrated aq. HI;; washing with concentrated aq. HI and removing H2O and HI over P2O5 in vacuum;;
