in benzene addition of a solution of 17.5 g twice sublimed I2 to a solution of 10 g Bi triphenyle in dry benzene;; filtration and washing the precipitate with benzene; removing the benzene in a vacuum desiccator over paraffine shavings;;
in neat (no solvent) byproducts: Al2S3; heating a mixture of molten AlI3 and Bi2S3 in an evacuated tube at 230°C for 48 hours;; sublimation in vacuum at 400°C;;
参考文献
Bulletin de la Societe Chimique de France, , p. 1192 - 1193
