tin(ll) chloride in hydrogenchloride SnCl2 soln. in HCl is satd. with iodine; addn. of a hydrochloric soln. of Bi2O3;; product is dried over CaCl2, heated below its melting temperature in an evacuated glass tube and sublimated in a stream of CO2 and H2;;
tin(ll) chloride in hydrogenchloride SnCl2 soln. in HCl is satd. with iodine; addn. of a BiOCl soln.;; product is dried over CaCl2, heated below its melting temperature in an evacuated glass tube and sublimated in a stream of CO2 and H2;;
in neat (no solvent) product sublimes while heating the mixture of the starting material;; heating a short time in a water bath to remove excess of iodine;;
参考文献
Journal of the Chemical Society, , vol. 67, p. 90 - 90
Annalen der Physik (Weinheim, Germany), , vol. 99, p. 470 - 470
