in neat (no solvent)
slow addition of BrF3 to icy cold CI4, reaction with inflammation;;
参考文献
Banks, A. A.; Emeleus, H. J.; Haszeldine, R. N.; Kerrigan, V.
Journal of the Chemical Society, 1948 , p. 2188 - 2190
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Gmelin Handbook: C: MVol.D2, 4.1.4.6, page 281 - 283
in neat (no solvent)
large excess of BrF3 is added to LiCl (quartz vessel); reaction is complete by heating to 120°C after few min.;; impurities: traces of Cl2 and Br2;;
参考文献
Sharpe, A. G.; Emeleeus, H. J.
Journal of the Chemical Society, 1948 , p. 2135 - 2138
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Gmelin Handbook: Li: SVol., 71, page 305 - 307
