in hydrogen fluoride HF (liquid); absence air and moisture; distn. of HF onto mixt. of equimolar amts. of BrF5 and water (-196°C), standing at -63°C for 1h, then at-78° for 2 d; removal of volatiles (-72°C, vac.); Raman spectroscopy;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1539 - 1546
