in neat (no solvent) absence of air and moisture; distn. of excess of BrF5 on IO2F3, warming to -18°C then to room temp. (40 min); product mixt. not sepd., detd. by (19)F NMR and Raman spectroscopy;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1539 - 1546