in neat (no solvent) large excess of BrF3 is added to LiCl (quartz vessel); reaction is complete by heating to 120°C after few min.;; impurities: traces of Cl2 and Br2;;
Cavell, R. G.; Clark, H. C.
Journal of the Chemical Society, 1962 , p. 2692 - 2698
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Gmelin Handbook: V: MVol.B1, 67, page 187 - 190
Sharp, D. W. A.
Journal of the Chemical Society, 1957 , p. 3761 - 3764
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Gmelin Handbook: Na: SVol.3, 3.3.4, page 1186 - 1188
in neat (no solvent) reaction of Ta-KCl mixtures (1:1) with BrF3;;
参考文献
Gutmann, V.; Emeleus, H. J.
Journal of the Chemical Society, 1950 , p. 1046 - 1050
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Gmelin Handbook: Ta: MVol.B2, 118, page 268 - 270
in not given a soln. of KBrF4 was treated with BrF2*TaF6 in BrF3;;
参考文献
Gutmann, V.; Emeleus, H. J.
Journal of the Chemical Society, 1950 , p. 1046 - 1050
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Gmelin Handbook: Ta: MVol.B2, 118, page 268 - 270
Banks, A. A.; Emeleus, H. J.; Haszeldine, R. N.; Kerrigan, V.
Journal of the Chemical Society, 1948 , p. 2188 - 2190
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Gmelin Handbook: C: MVol.D2, 4.1.2.7.8.3, page 243 - 243
