3-(甲氧羰基)-2,2,6,6-四甲基-4-氧代-合成路线 (共 3 条)
反应条件
1: 1-oxyl-2,2,6,6-tetramethylpiperidin-4-one; carbon dioxide With potassium phenolate in N,N-dimethyl-formamide
T=20°C; 2 h;
2: diazomethane in diethyl ether
参考文献
Wright, Karen; Crisma, Marco; Toniolo, Claudio; Toeroek, Roland; Peter, Antal; Wakselman, Michel; Mazaleyrat, Jean-Paul
Tetrahedron Letters, 2003 , vol. 44, # 16 p. 3381 - 3384
反应条件
1: potassium phenoxide / dimethylformamide / 2 h / Ambient temperature; molar ratio of 1:2 of substrate and potassium phenoxide
2: diethyl ether
View Scheme
参考文献
Mori; Ohara; Kwan
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 11 p. 3178 - 3183
反应条件
in diethyl ether
Yield given;
参考文献
Mori; Ohara; Kwan
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 11 p. 3178 - 3183