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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-苯基-1H-吲唑
合成路线
（共 23 条）
1415581-18-8
→
反应条件
7788-69-4
1-苯基-1H-吲唑
反应条件
bis(acetylacetonate)nickel(II); 1,1,3,3-tetramethyldisiloxane; trimethylaluminum; tri-cyclo-hexyl-phosphine in toluene T=130°C; 24 h; Inert atmosphere;
参考文献
Patra, Tuhin; Agasti, Soumitra; Akanksha; Maiti, Debabrata
Chemical Communications, 2013 , vol. 49, # 1 p. 69 - 71
271-44-3
吲唑
+
934-56-5
三甲基(苯基)锡
→
反应条件
7788-69-4
1-苯基-1H-吲唑
反应条件
pyridine; copper diacetate in 1,4-dioxane T=80°C; Arylation; 48 h;
参考文献
Lam, Patrick Y.S.; Clark, Charles G.; Saubern, Simon; Adams, Jessica; Averill, Kristin M.; Chan, Dominic M. T.; Combs, Andrew
Synlett, 2000 , # 5 p. 674 - 676
100-63-0
苯肼
→
反应条件
7788-69-4
1-苯基-1H-吲唑
反应条件
1: 100 percent / 1-methyl-pyrrolidin-2-one / 0.17 h / 160 °C / microwave irradiation 2: 94 percent / K2CO3; (1R,2R)-1,2-cyclohexanebis(methylamine) / CuI / 1-methyl-pyrrolidin-2-one / 0.17 h / 160 °C / microwave irradiation View Scheme
参考文献
Pabba, Chittari; Wang, Hong-Jun; Mulligan, Susan R.; Chen, Zhen-Jia; Stark, Todd M.; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 44 p. 7553 - 7557
271-44-3
吲唑
+
28899-97-0
→
反应条件
3682-71-1
+
7788-69-4
1-苯基-1H-吲唑
反应条件
copper diacetate; N,N,N',N'-tetramethylguanidine in tetrahydrofuran T=50°C; Arylation; 7 h;
参考文献
Fedorov, Alexey Yu; Finet, Jean-Pierre
Tetrahedron Letters, 1999 , vol. 40, # 14 p. 2747 - 2748
6630-33-7
邻溴苯甲醛
→
反应条件
7788-69-4
1-苯基-1H-吲唑
反应条件
1: 100 percent / 1-methyl-pyrrolidin-2-one / 0.17 h / 160 °C / microwave irradiation 2: 91 percent / K2CO3; (1R,2R)-1,2-cyclohexanebis(methylamine) / CuI / 1-methyl-pyrrolidin-2-one / 0.17 h / 160 °C / microwave irradiation View Scheme
参考文献
Pabba, Chittari; Wang, Hong-Jun; Mulligan, Susan R.; Chen, Zhen-Jia; Stark, Todd M.; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 44 p. 7553 - 7557
3433-80-5
2-溴溴苄
→
反应条件
7788-69-4
1-苯基-1H-吲唑
反应条件
1: LHMDS 2: 58 percent / dppf; tBuONa / Pd(OAc)2 / dioxane / 15 h / 90 °C View Scheme
参考文献
Song, Jinhua J.; Yee, Nathan K.
Tetrahedron Letters, 2001 , vol. 42, # 16 p. 2937 - 2940
26260-02-6
2-碘苯甲醛
→
反应条件
7788-69-4
1-苯基-1H-吲唑
反应条件
1: 100 percent / 1-methyl-pyrrolidin-2-one / 0.17 h / 160 °C / microwave irradiation 2: 94 percent / K2CO3; (1R,2R)-1,2-cyclohexanebis(methylamine) / CuI / 1-methyl-pyrrolidin-2-one / 0.17 h / 160 °C / microwave irradiation View Scheme
参考文献
Pabba, Chittari; Wang, Hong-Jun; Mulligan, Susan R.; Chen, Zhen-Jia; Stark, Todd M.; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 44 p. 7553 - 7557
89-98-5
2-氯苯甲醛
→
反应条件
7788-69-4
1-苯基-1H-吲唑
反应条件
1: 100 percent / 1-methyl-pyrrolidin-2-one / 0.17 h / 160 °C / microwave irradiation 2: 87 percent / K2CO3; (1R,2R)-1,2-cyclohexanebis(methylamine) / CuI / 1-methyl-pyrrolidin-2-one / 0.17 h / 160 °C / microwave irradiation View Scheme
参考文献
Pabba, Chittari; Wang, Hong-Jun; Mulligan, Susan R.; Chen, Zhen-Jia; Stark, Todd M.; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 44 p. 7553 - 7557
59-88-1
盐酸苯肼
+
90-02-8
水杨醛
→
反应条件
7788-69-4
1-苯基-1H-吲唑
反应条件
in ethanol Heating;
参考文献
Lokhande; Raheem, Abdul; Sabale; Chabukswar; Jagdale
Tetrahedron Letters, 2007 , vol. 48, # 39 p. 6890 - 6892
98-80-6
苯硼酸
→
反应条件
7788-69-4
1-苯基-1H-吲唑
反应条件
1: 94 percent / Cu(OAc)2; pyridine / CH2Cl2 / 28 h / 20 °C 2: 89 percent / KOH / ethanol / 6 h / Heating View Scheme
参考文献
Hari, Yoshiyuki; Shoji, Yoshimichi; Aoyama, Toyohiko
Tetrahedron Letters, 2005 , vol. 46, # 21 p. 3771 - 3774
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