1,4,7,10-四氧杂环十三烷-12-醇合成路线 (共 3 条)
反应条件
palladium 10 on activated carbon; hydrogen in methanol
T=23°C;
参考文献
Ghosh, Aran K.; Gemma, Sandra; Baldridge, Abigail; Wang, Yuan-Fang; Kovalevsky, Andrey Yu.; Koh, Yashiro; Weber, Irene T.; Mitsuya, Hiroaki
Journal of Medicinal Chemistry, 2008 , vol. 51, # 19 p. 6021 - 6033
反应条件
lithium boron tetrafluoride; boron trifluoride diethyl etherate in 1,4-dioxane
参考文献
Shabanov, A. L.; Ismiev, I. I.; Magerramova, L. M.; Elchiev, A. B.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 2 p. 251 - 254
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 284 - 288
反应条件
lithium
1.) dioxane, 2.) dioxane, reflux, 20 h; Yield given. Multistep reaction;
参考文献
Ikeda; Katayama; Tsuchiya; Okahara
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2473 - 2475