in neat (no solvent) distillation of BrI or passing BrI in a H2 stream to crystalline Si near red heat;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 1447 - 1449
Full Text Show Details
Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
in neat (no solvent) distillation of BrI or passing BrI in a H2 stream to crystalline Si near red heat;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 1447 - 1449
Full Text Show Details
Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
in neat (no solvent, gas phase)
Kinetics; react. in a flowing-afterglow reactor, carrier gas Ar (flow rate 0.05 mol/min, 1.5 Torr, 50°C); not isolated;
参考文献
Zhang, Fu Min; Oba, D.; Setser, D. W.
Journal of Physical Chemistry, 1987 , vol. 91, # 5 p. 1099 - 1114
in chloroform
byproducts: C6H5I; a soln. of IBr is added dropwise with vigorous stirring to a soln. of Sn-compd. at room temp., after decolourisation the mixt. is refluxed for 2 h (N2); mixt. is concd. by distn. at reduced pressure (10 mmHg), to residue petroleum ether is added, kept at 0°C, ppt. is sepd. after 24 h, washed (petroleum ether) and dried at 20°C/10 mmHg, elem. anal.;
参考文献
Srivastava, P.C.; Srivastava, S.K.; Sharma, Suman B.
Canadian Journal of Chemistry, 1985 , vol. 63, p. 329 - 331
