in neat (no solvent)
melting a mixt. of 51.1 mol-percent PBr3 and 48.9 mol-percent IBr; react. of the prod. with PBr3 then with CS2;; drying the residue at 50 °C in a stream of CO2;;
参考文献
Fialkov, Ya. A.; Kuz'menko, A. A.
Zh. obshch. Khim., 1949 , vol. 19, p. 1645 - 1652
C. A., 1950 , p. 1354
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Gmelin Handbook: P: MVol.C, 232, page 531 - 533
