in THF-d8 (tetrahydrofuran-d8) Sonication; (Ar); sonication of a mixt. of metal complexes in THF-d8 for 10 min in an NMR tube; not isolated, detected by NMR;
in neat (no solvent) mixt. of metal and I2 was heated to the deflagration point of the mixt. in vac.; excess of I2 was evacuated, tube was filled with Ar, solidified metal part was removed, elem. anal.; metal triiodide was deposited on the wall of tube;
参考文献
Zeitschrift fur Anorganische und Allgemeine Chemie, , vol. 628, # 3 p. 699 - 702
