ClF3 admitting into reaction vessel (Pyrex glass) with silicon (initial p(ClF3)=38300 Pa, reaction duration 1-2 min); gravimetric and volumetric monitoring after 10 min at room temp.;
参考文献
Garabin, V. F.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1979 , vol. 24, p. 1606 - 1608
Zhurnal Neorganicheskoi Khimii, 1979 , vol. 24, p. 2892 - 2896
byproducts: Cl2, SO2F2; in an autoclave, warming from -196 to -78°C, then to 20°C;
参考文献
Schack, C. J.; Wilson, R. D.
Inorganic Chemistry, 1970 , vol. 9, p. 311 - 314
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Gmelin Handbook: S: SVol.3, 2.1.8.9.5.3, page 195 - 195
byproducts: Cl2; room temp.; 200 Torr; metallic Se is used;
参考文献
Pitts, J. J.; Jache, A. W.
Inorganic Chemistry, 1968 , vol. 7, p. 1661 - 1663
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Gmelin Handbook: Se: SVol.A3, 17.3.2, page 292 - 293
