ClSO2F (sulfuryl chloride fluoride) in not given SO2ClF and ClF were condensed onto (SCl)2NAsF6, mixt. was warmed to room temp. with srirring, 5 h; volatiles were removed, products were not isolated; products were analized by IR;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1961 - 1968
in neat (no solvent) The reactor with SF3N and ClF was warmed from -196°C to -78°C over 14 h; addn. of F2, warming; pumped through traps at -78, -115, and -196°C;
