ClF3 admitting into reaction vessel (Pyrex glass) with silicon (initial p(ClF3)=19500 Pa, reaction duration 1-2 min); gravimetric and volumetric monitoring after 10 min at room temp.;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 24, p. 1606 - 1608
Zhurnal Neorganicheskoi Khimii, , vol. 24, p. 2892 - 2896
ClF3 admitting into reaction vessel (Pyrex glass) with silicon (initial p(ClF3)=54300 Pa, reaction duration 1-2 min); gravimetric and volumetric monitoring after 10 min at room temp.;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 24, p. 1606 - 1608
Zhurnal Neorganicheskoi Khimii, , vol. 24, p. 2892 - 2896
ClF3 admitting into reaction vessel (Pyrex glass) with silicon (initial p(ClF3)=38300 Pa, reaction duration 1-2 min); gravimetric and volumetric monitoring after 10 min at room temp.;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 24, p. 1606 - 1608
Zhurnal Neorganicheskoi Khimii, , vol. 24, p. 2892 - 2896
F2 in neat (no solvent) dry air atmosphere; heating Bi and BiF3 (F2 stream, 450-500°C);
参考文献
Popov, A. I.; Scharabarin, A. V.; Sukhoverkhov, V. F.; Tchumaevsky, N. A.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1989 , vol. 576, p. 242 - 254
