in tetrachloromethane Ar-atmosphere; dropwise addn. of ICl to equimolar amt. of Sn-compd., stirring for 5 min; solvent removal, distn. (108-111°C, 20 mm Hg);
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Al-Juaid, Salih S.; Al-Rawi, Mustafa; Eaborn, Colin; Hitchcock, Peter B.; Smith, J. David
Journal of Organometallic Chemistry, 1998 , vol. 564, # 1-2 p. 215 - 226
Folaranmi, A; McLean, R. A. N.; Wadibia, N.
Journal of Organometallic Chemistry, 1974 , vol. 73, p. 59 - 66
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.5.4.3, page 103 - 104
in carbon disulfide under N2, dropwise addn. of a Br2/CS2 soln. to a vigorously stirred soln. of P4/CS2 reaction of P4 with ICl (molar ratio (1.75:1.5), further Products: PCl3, PCl2I, PClI2, PI3; not isolated, identified by 31P-NMR spectroscopy;
参考文献
Tattershall, Bruce W.; Kendall, Nigel L.
Polyhedron, 1994 , vol. 13, p. 1517 - 1522
Gutmann, V.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1951 , vol. 264, p. 169 - 173
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Gmelin Handbook: Se: SVol.A3, 17.3.2, page 292 - 293
